王春红1 兰红2
(1.湖北省药品检验所 2.湖北民康药业有限公司)
摘要: 目的:建立舒心口服液中黄芪甲苷薄层扫描法测定含量方法。方法:采用双波长薄层法扫描法(λs=530nm,λR=700nm)进行测定舒心口服液中黄芪甲苷的含量 结果:黄芪甲苷在1.01-8.08μg范围内呈良好的线性关系,平均回收率=98.46%,RSD=3.89%,结论:该方法简便、结果准确、重现性好,可用于舒心口服液的质量控制
关键词:薄层扫描法; 舒心口服液; 黄芪甲苷
Determination of Astragalosid I in shuxing koufuye by dual wavelength TLC-Scanning
Wangchunhong1 LanHong2
(1.Hubei provincial Institute for Drug Contorl ,wuhan 430064,chain
2.Hubei minkang yaoye youxian gongshi yichang 443000 ,chain)
Abstract: Objiective :To establish a TLC-scanning for the quantitative determination of Astragalosid I. in shuxing Koufuye .Methods :Determination of Astragalosid I in shuxing koufuye by dual wavelength TLC-Scanning Results :Astragaloside I showed good linear relationship in the concentration range of 1.08-8.08vg;and the average recovery was up to 98.46%,RSD was 3.89%. Conclusion: the method is simple ,the result is accurate and reproducibility is good and be used as the quality control of shuxing koufuye.
Key word: TLC-Scanning; shuxing Koufuye ; Astragalosid I. 资料来自:中国药师-专业站 |