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双波长薄层扫描法测定舒心口服液中黄芪甲苷的含量

阅读: 时间: 2005-7-2 9:51:00

王春红1       兰红2

1.湖北省药品检验所     2.湖北民康药业有限公司

摘要目的:建立舒心口服液中黄芪甲苷薄层扫描法测定含量方法。方法:采用双波长薄层法扫描法(λs=530nm,λR=700nm)进行测定舒心口服液中黄芪甲苷的含量  结果黄芪甲苷在1.01-8.08μg范围内呈良好的线性关系,平均回收率=98.46%,RSD=3.89%,结论:该方法简便、结果准确、重现性好,可用于舒心口服液的质量控制

关键词薄层扫描法;  舒心口服液;    黄芪甲苷

Determination of Astragalosid I in shuxing koufuye by dual wavelength TLC-Scanning

             Wangchunhong1        LanHong2

       (1.Hubei provincial Institute for Drug Contorl ,wuhan 430064,chain

        2.Hubei minkang yaoye youxian gongshi yichang 443000 ,chain)

Abstract: Objiective :To establish a TLC-scanning for the quantitative determination of Astragalosid  I. in shuxing Koufuye  .Methods :Determination of Astragalosid I in shuxing koufuye by dual wavelength TLC-Scanning  Results :Astragaloside I  showed good linear relationship in the concentration range of 1.08-8.08vg;and the average recovery was up to 98.46%,RSD was 3.89%.  Conclusion: the method is simple ,the result is accurate and reproducibility is good and be used as the  quality control of shuxing koufuye.

 Key word: TLC-Scanning;  shuxing Koufuye ;  Astragalosid I.

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