张丽辉 冯海龙 徐玲(湖北省药品检验所 武汉 430064)
摘 要 目的:建立垂阴茶糖浆岩白菜素的测定方法,方法:λs=275nm,λR=320nm,用薄层色谱法测定岩白菜素的含量。结果:岩白菜素在0.505~3.030μg范围内线性关系良好(r=0.999 9),平均回收率为96.52%。RSD=0.44%。结论:该法灵敏度高,重现性好,可用于该制剂中岩白菜素的含量测定及质量控制。
关键词:垂阴茶糖浆;薄层色谱扫描法;岩白菜素
Content Determination of Bergenin in Chuiyincha Syprup by TLC Scanning
Zhang Lihui Fong Hailong Xu Ling
(HUBEI RPOVINCIAL INSTITVTE FOR DRUGCONTROL, Wuhan 430064 ,P.R China).
ABSTRACT Objective:To determine the content of Bergenin Ain chuiyincha Tangjiang.
Method:TLC scanning method was used Result: The linear range was within 0.505~3.030μg(r=0.9999 n=5)。 The average recovery of Bergenin was 96.52%. RSD=0.44% .
Conclusion:The method is simple,rapid and reproducible and TLC scanning is a good method for quality control of chuiyincha Tangjiang. KEY WORDS: TLC scanning; Bergenin chuiyincha Tangjiang.资料来自:中国药师-专业站 |