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薄层扫描法测定垂阴茶糖浆中岩白菜素的含量测定

阅读: 时间: 2005-7-4 13:10:00

张丽辉 冯海龙 徐玲(湖北省药品检验所 武汉 430064)

 

摘  要  目的建立垂阴茶糖浆岩白菜素的测定方法,方法:λs275nm,λR320nm,用薄层色谱法测定岩白菜素的含量。结果:岩白菜素在0.5053.030μg范围内线性关系良好(r=0.999 9),平均回收率为96.52%RSD0.44%结论该法灵敏度高,重现性好,可用于该制剂中岩白菜素的含量测定及质量控制。

关键词:垂阴茶糖浆;薄层色谱扫描法;岩白菜素

Content Determination of Bergenin in Chuiyincha Syprup by TLC Scanning

Zhang Lihui Fong Hailong Xu Ling

(HUBEI RPOVINCIAL INSTITVTE FOR DRUGCONTROL, Wuhan 430064 ,P.R China).

ABSTRACT Objective:To determine the content of Bergenin Ain chuiyincha Tangjiang.

Method:TLC scanning method was used Result: The linear range was within 0.5053.030μg(r=0.9999 n=5)。 The average recovery of Bergenin was 96.52%. RSD=0.44% .

Conclusion:The method is simple,rapid and reproducible and TLC scanning is a good method for quality control of chuiyincha Tangjiang.

KEY WORDS: TLC scanning; Bergenin chuiyincha Tangjiang.

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