洪美华 李晓茵 单当当 (汕尾市药品检验所 广东汕尾 516600)
摘 要 目的：制订橘红枇杷片的质量标准。方法：采用薄层色谱法对方中枇杷叶、陈皮进行定性鉴别；采用HPLC法测定化橘红中柚皮苷的含量。
结果：所采用的薄层色谱鉴别方法专属性强，阴性对照无干扰；平均回收率100.7%,RSD为1.3%。结论：所建立的方法简便、准确、专属性、重现性好, 可作为该制剂的质量控制。
关键词 橘红枇杷片；柚皮苷；高效液相色谱法
中图分类号：TQ460.7+ 2
文献标识码：A
文章编号：1008-049X(2007)08-0771-02
Study on Quality Standard for Juhongpipa Tablets
Hong Meihua, Li Xiaoyin，Shan Dangdang(Shanwei Institute for Drug Control,Guangdong，Shanwei 516600,China)
ABSTRACT Objective: To establish the quality standard for Juhongpipa Tablets.Method: The Folium eriobotryae and Pericarpium citri reticulatae were identified by TLC, the content of narigin was determined by HPLC.Result: The spots in the TLC were clear and distinguished well. The average recovery was 100.7％and RSD was 1.3％.Conclusion: The method is simple, accurate and specific. It can be used for the quality control of Juhongpipa Tablets.
KEY WORDS Juhongpipa Tablets；Narigin；HPLC
参 考 文 献
1 卫生部药品标准［S］.WS3-B-0688-91
2 中国药典［S］.2005年版. 一部. 132,51 资料来自:中国药师-专业站 |